王志兵

个人信息

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教授     博士生导师     硕士生导师

教师英文名称:Zhibing Wang

教师拼音名称:wangzhibing

出生日期:1982-01-12

电子邮箱:

入职时间:2008-04-01

所在单位:长春工业大学化学与生命科学学院

职务:副院长

学历:研究生(博士)毕业

办公地点:南湖校区材料楼311

性别:男

联系方式:0431-85716470

学位:博士学位

在职信息:在职

毕业院校:吉林大学

学科:应用化学
生物学其他专业
分析化学
学术荣誉:
2018    学科带头人
2018    教学名师
曾获荣誉:
2023-04-26    吉林省高层次D类人才
2020-12-25    吉林省第二届高等学校教学新秀
2019-11-30    吉林省大学生生命科学竞赛优秀指导教师
2018-10-14    第十一届全国大学生创新创业年会优秀指导教师
2023-08-30    CULSC第八届全国大学生生命科学竞赛指导教师一等奖
2018-05-16    吉林省自然科学学术成果奖一等奖
2010-12-30    吉林省科学技术进步奖三等奖
2010-12-20    长春市科学技术进步奖三等奖
2008-06-08    吉林省高校科学技术研究优秀成果奖二等奖
2007-12-26    吉林省科学技术发明奖二等奖

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(外博SCI)Simultaneous determination of nucleosides and their bases in Cordyceps sinensis and its substitutes by matrix solid-phase dispersion extraction and HPLC
发布时间:2021-06-28  点击次数:

所属单位:化学与生命科学学院
教研室:食品教研室
发表刊物:Journal of Separation Science
项目来源:其他课题
关键字:Cordyceps sinensis / HPLC / Matrix solid-phase dispersion / Nucleobases
摘要:Nine nucleosides and nucleobases, including uracil, adenine, thymine, uridine, adenosine,thymidine, cytidine, guanosine, and cordycepin in natural Cordyceps sinensis, cultured Cordyceps mycelia, and Cordyceps fruiting bodies were extracted by matrix solid-phase dispersion (MSPD) and determined by HPLC. The experimental conditions for the MSPD extraction were optimized. Florisil was used as dispersant, petroleum ether as washing solvent, and methanol as elution solvent. The Florisil-to-sample ratio was selected to be 4:1 and no additional clean-up sorbent was needed. The calibration curves had good linear relationships (r > 0.9997). The LOD and LOQ were in the range of 12 ∼ 79 and 41 ∼ 265 ng/mL,respectively. The intra- and interday precision were lower than 8.3%. The recoveries were between 61.5 and 93.2%. The present method consumed less sample compared with ultrasonic extraction and heating reflux extraction (HRE). The extraction yields obtained by using the present method are much higher than those obtained by UE and comparable to those obtained by HRE.
合写作者:李娜,王敏,王月,杜琳,季晓峰,于爱民,张寒琦,邱芳萍
第一作者:王志兵
论文类型:期刊论文
卷号:36
期号:14
页面范围:2
字数:1
是否译文:否
发表时间:2013-07-01