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Affiliation of Author(s):化学工程学院
Teaching and Research Group:化学工程学院
Journal:Applied Mechanics and Materials
Funded by:省、市、自治区科技项目
Key Words:HBS,1,4-butanediol,Pine-nut shell Lignin,Lignin-PEG-PAPI
Abstract:By the method of high boiling solvent (HBS), HBS-lignin has been separated from pine-nut hull with 1,4-butanediol solution as solvent, and characterized by GPC, IR, 1HNMR and TG. The optimal conditions are described as: the ratio of solid raw material to solvent (g:mL) in 1:12, the amount of catalyst in 6%, the reaction time for 2 hrs, reaction temperature at 200°C, and 90% of 1,4-butanediol as the solvent, and the yield of lignin up to 70%. The hydroxyl value of obtained HBS-lignin is about 197.2mgKOH/g. Furthermore, the HBS-lignin replaces the partial PEG400 to employ the synthesis of lignin-PEG-PAPI. The experimental results indicate that mechanical properties and solvent resistance of lignin-PEG-PAPI are apparently improved with comparison to the PEG-PAPI.
Co-author:贾俊,曲玉超,高月,袁永鹏,王凯凯,杨帆,吴广峰
First Author:wuguangfeng
Indexed by:Journal paper
Volume:320
Page Number:1
Number of Words:1
ISSN No.:1662-7482
Translation or Not:no
Date of Publication:2013-05-07
