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【外博SCI】Microstructural differences between electrospun alumina borate nanofibers prepared by solutions with different PVP contents
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所属单位:材料科学工程学院
发表刊物:Ceramics International
项目来源:国家科技部
关键字:alumina borate; nanofibers; electrospinning; microstructure; polyvinyl pyrrolidone
摘要:Alumina borate nanofibers were fabricated by electrospinning combined with sol-gel method using aluminum acetate (Al(OH)2(OOCCH3)•1/3H3BO3, stabilized with boric acid) and polyvinyl pyrrolidone (PVP) as raw materials. As-spun composite nanofibers were electrospun from the spinning solutions prepared with different PVP contents. The as-spun nanofibers were calcined at 1000 ℃ and the microstructures of the calcined nanofibers were investigated. The results showed that with the content of PVP increased, the diameters of the alumina borate nanofibers increased, and the temperatures at which the Al4B2O9 phase formed and Al4B2O9 transformed to Al18B4O33 also increased. However, the crystallinity of the calcined nanofibers decreased with the increase of the PVP content. The grains became smaller and more uniform due to the increasing amount of voids and cracks generated by the decomposition of PVP.
合写作者:刘文胜,王娟,徐书恒,刘竝,刘继进,马运柱
第一作者:宋晓雷
论文类型:期刊论文
卷号:43
期号:13
页面范围:1
ISSN号:0272-8842
是否译文:否
发表时间:2017-04-27